N-Benzylaniline

Imikoreshereze y'ibicuruzwa:

Kugirango hamenyekane aside sulfonique, synthesis organic.

uburyo bwo kubyaza umusaruro:

Bikomoka kuri kondegene ya benzyl chloride na aniline.Kuvanga no kuvanga sodium bicarbonate, amazi na aniline, gushyushya 90-95 ° C, hanyuma ukongeramo buhoro buhoro chloride ya benzyl.Reba kuri 90-95 ° C kuri 3h.Gukonjesha no kuyungurura.Akayunguruzo karatandukanijwe, kandi urwego kama rwogejwe na brine yuzuye hanyuma rwumishwa hejuru ya sodium sulfate ya anhydrous.Noneho gucamo vacuum, gukusanya 81 ℃ (1.6kPa) agace kugirango ugarure aniline, 170-190 ℃ (1.6kPa) gukonjesha agace, gukomera kugirango ubone benzyl aniline.Irashobora kongera guhindurwa uhereye kuri peteroli ether mugihe cyo kwezwa.Umusaruro uri hejuru ya 80%.